|本期目录/Table of Contents|

[1]刘正明a,b,刘建华a,等. 黄芩苷Al(Ⅲ)络合染料的制备及其真丝绸染色[J].浙江理工大学学报,2011,28(02):155-159.
　LIU Zheng ming,LIU Jian hua,YU Zhi cheng. Preparation of BaicalinAl(Ⅲ) Complex Dyes and Dyeing of Silk Fabric[J].Journal of Zhejiang Sci-Tech University,2011,28(02):155-159.
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 黄芩苷Al(Ⅲ)络合染料的制备及其真丝绸染色()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第28卷
期数:
2011年02期
页码:
155-159
栏目:
(自科)纺织与服装工程
出版日期:
2011-04-30

文章信息/Info

Title:
 Preparation of BaicalinAl(Ⅲ) Complex Dyes and Dyeing of Silk Fabric
文章编号:
16733851 (2011) 02015505
作者:
 刘正明a; b;  刘建华a; b;  余志成a; b
 浙江理工大学, a. 生态染整技术教育部工程研究中心; b. 先进纺织材料与制备技术教育部重点实验室， 杭州 310018
Author(s):
 LIU Zhengming;  LIU Jianhua;  YU Zhicheng
 Zhejiang SciTech University, a. Engineering Research Center for EcoDyeing & Finishing of Textiles, Ministry of Education; b. The Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Hangzhou 310018, China
关键词:
 ; 天然染料;  黄芩苷Al(Ⅲ)络合染料;  染色;  丝绸
分类号:
TS193. 21
文献标志码:
A
摘要:
     为提高黄芩天然染料染色的色深及色牢度，对黄芩苷Al(Ⅲ)络合染料的制备工艺进行了研究。采用FTIR对络合物的结构进行表征，并将络合染料直接应用于真丝织物染色。实验结果表明：黄芩苷Al(Ⅲ)络合染料制备的最佳工艺参数为：n(黄芩苷)∶n(Al3+)=2∶1，pH值为5，反应温度40℃，时间30 min；由红外谱图可知：黄芩苷分子4位的羰基和5位的酚羟基与Al3+发生了配位反应；黄芩苷络合染料染色的真丝织物具有较高的K/S值和色牢度。

参考文献/References:

 ［1］ 孙鑫, 程万里. 黄芩对真丝织物染色的研究［J］. 丝绸, 2002(2): 1113.
［2］ Gao Peipei, Yang Xing, Yu Zhicheng. The extraction of antibacterial components of scutellaria baicalinsis georgi and their application on silk fabric［C］//Zhejiang SciTech University. Proceedings of the International Conference on Advanced Textile Materials & Manufacturing Technology. Hang Zhou: Zhejiang University Press, 2008: 220225.
［3］ 李慧玲, 吴明华, 林鹤鸣. 茶多酚铜络合物的合成及其抗菌、消臭性能研究［J］. 浙江理工大学学报, 2008, 25(3): 266270.
［4］ Armida Torreggiani. Copper(Ⅱ)Quercetin complexes in aqueous solutions: spectroscopic and kinetic properties［J］. Journal of Molecular Structure, 2005(744747): 759766.
［5］ 吴魏, 周奕含, 刘志强, 等. 黄芩苷与铝离子配合物的电喷雾质谱研究［J］. 分析化学研究简报, 2005, 33(5): 683686.
［6］ 李思睿, 董慧茹, 毕鹏禹. 黄芩苷Fe(Ⅱ)配合物的合成与表征［J］. 北京化工大学学报, 2006, 33(2): 97100.

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备注/Memo

备注/Memo:
 收稿日期： 2010-09-09
作者简介： 刘正明（1985-），女，新疆库尔勒人，硕士研究生，主要从事生态纺织品与绿色染整技术研究。
通讯作者： 余志成，电子邮箱：yuzhicheng8@yahoo.com.cn
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