|本期目录/Table of Contents|

[1]黎浩,翟欣,刘勇,等.加速炭化对丝织品结构及稳定同位素的影响[J].浙江理工大学学报,2023,49-50(自科五):589-594.
 LI Hao,ZHAI Xin,LIU Yong,et al.Effects of accelerated carbonization on the structure and stable isotopes of silk fabrics[J].Journal of Zhejiang Sci-Tech University,2023,49-50(自科五):589-594.
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加速炭化对丝织品结构及稳定同位素的影响()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第49-50卷
期数:
2023年自科第五期
页码:
589-594
栏目:
出版日期:
2023-09-24

文章信息/Info

Title:
Effects of accelerated carbonization on the structure and stable isotopes of silk fabrics
文章编号:
1673-3851 (2023) 09-0589-06
作者:
黎浩翟欣刘勇贾丽玲彭志勤
1.浙江理工大学材料科学与工程学院,杭州 310018;2.中国丝绸博物馆,杭州 310002
Author(s):
LI Hao ZHAI Xin LIU Yong JIA Liling PENG Zhiqin
1.School of Materials Science & Engineering, Zhejiang Sci-Tech University, Hangzhou 310018, China;2.China National Silk Museum, Hangzhou 310002, China
关键词:
丝织品炭化二级结构稳定同位素 形貌
分类号:
TS141
文献标志码:
A
摘要:
为探究丝织品炭化前后的形貌、结构及稳定同位素比值的变化情况,采用热老化试验箱对现代丝织品进行人工加速炭化试验,利用扫描电镜、红外光谱仪和稳定同位素质谱仪对样品进行表征。结果表明:丝织品在200 ℃炭化条件下0.5 h后变黄并最终变黑;炭化24.0 h后,蚕丝纤维的强度降低,直径明显减小,同时 β 折叠结构会向 α 螺旋结构和无规卷曲结构转变;丝织品中的碳、氮稳定同位素比值在炭化后均被富集,氢、氧稳定同位素被贫化。该研究可以为丝织品的产地溯源提供一定科学依据。

参考文献/References:

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5Dan M P, Zhang B, Martin G J. Determination of the geographical origin of wine using joint analysis of elemental and isotopic composition. II: Differentiation of the principal production zones in france for the 1990 vintageJ. Journal of the Science of Food and Agriculture, 1995, 67(1): 113-123.

6Von Holstein I C C, Rogers P W, Craig O E, et al. Provenancing archaeological wool textiles from medieval northern europe by light stable isotope analysis (δ13 C, δ15 N, δ 2H)J. PLOS ONE, 2016, 11(10):113-123.

7Knaller R, StrbeleF. The heritage of Tang dynasty textiles from the Famen Temple, Shaanxi, China: Technological and stable isotope studiesJ. Studies in Conservation, 2014, 59(S1): 62-65.

8Zhang X, Gong D, Gong Y. Insight into the orientation behavior of thermal-aged and historic silk fabrics by polarized FTIR microspectroscopyJ. Journal of Cultural Heritage, 2019, 38: 53-63.

9Vilaplana F, Nilsson J, Sommer D V P, et al. Analytical markers for silk degradation: comparing historic silk and silk artificially aged in different environmentsJ. Analytical and Bioanalytical Chemistry, 2015, 407(5): 1433-1449.

10]何宇杰, 彭志勤, 贾丽玲, . 碱老化对丝织物结构及稳定同位素比值的影响[J. 丝绸, 2022, 59(5): 14-19.

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备注/Memo

备注/Memo:
收稿日期: 2023-02-10
网络出版日期:2023-05-05
基金项目: 国家重点研发计划项目(2019YFC1521302);浙江省自然科学基金项目(LY19D030001);浙江省文物保护专项项目(2021015,2018012);甘肃省科技计划资助项目(20JR5RA052)
作者简介: 黎浩(1999-),男,江西九江人,硕士研究生,主要从事丝织品文物溯源的研究
通信作者: 彭志勤,E-mail:pengqiao6858@126.com
更新日期/Last Update: 2023-09-19