|本期目录/Table of Contents|

[1]张晓辉,胡英,黄飞桥,等.氧化亚铜准球形聚集体的合成及其抗菌性能[J].浙江理工大学学报,2023,49-50(自科六):682-690.
 ZHANG Xiaohui,HU Ying,HUANG Feiqiao,et al.Synthesis and antibacterial properties of cuprous oxide quasispherical aggregates[J].Journal of Zhejiang Sci-Tech University,2023,49-50(自科六):682-690.
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氧化亚铜准球形聚集体的合成及其抗菌性能()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第49-50卷
期数:
2023年自科第六期
页码:
682-690
栏目:
出版日期:
2023-11-10

文章信息/Info

Title:
Synthesis and antibacterial properties of cuprous oxide quasispherical aggregates
文章编号:
1673-3851 (2023) 11-0681-10
作者:
张晓辉胡英黄飞桥吕路明彭志勤颜志勇
1.浙江理工大学材料科学与工程学院,杭州 310018;2.嘉兴学院材料与纺织工程学院,浙江嘉兴 314000
Author(s):
ZHANG Xiaohui HU Ying HUANG Feiqiao LU Luming PENG Zhiqin YAN Zhiyong
1.School of Materials Science & Engineering, Zhejiang SciTech University, Hangzhou 310018, China; 2.College of Materials and Textile Engineering, Jiaxing University, Jiaxing 314000, China
关键词:
氧化亚铜准球形聚集体液相还原法废弃葡萄还原糖抗菌
分类号:
TQ131.2
文献标志码:
A
摘要:
以废弃葡萄果肉提取物(Waste grape pulp extract, WGPE)为还原剂,采用液相还原法将硫酸铜还原成氧化亚铜准球形聚集体(Cu2O-SA),借助傅里叶变换红外光谱仪、X射线薄膜衍射仪、X射线光电子能谱、扫描电子显微镜和场发射透射电子显微镜等表征分析Cu2O-SA的化学结构和形貌,测定反应条件对Cu2O-SA形貌和粒径的影响,并评价Cu2O-SA的抗菌效果。结果表明:以WGPE替代葡萄糖为还原剂或提高WGPE的浓度均有利于Cu2O-SA的合成;提高还原剂浓度和反应温度可使Cu2O-SA的粒径变小,粒径分布区间变窄,比表面积增大;Cu2O-SA是通过晶粒团聚生长并相互融合形成的多晶粉末,且随着生长时间的增加Cu2O-SA会发生聚集和表面重建;Cu2O-SA对金黄色葡萄球菌和大肠杆菌的最小抑菌质量浓度均在3.125~6.250 g/L。该研究对氧化亚铜纳米颗粒的合成和抗菌领域的应用具有指导意义。

参考文献/References:

1 Shahid M, Ali A, Khaleeq H, et al. Development of antimicrobial multifunctional textiles to avoid from hospitalacquired infections J . Fibers and Polymers, 2021, 22(11): 30553067.

2 Li M N, Chen Z F, Sun Y, et al. Preparation and antibacterial activity of graphene oxide/cuprous oxide/zinc oxide nanocomposite J . Materials Research Express, 2021, 8(12): 125003.

3 ]〖 JP2 Su Y M, Xu H L, Liao Z M, et al. Copperbased nanoparticles as antibacterial agents J . European Journal of Inorganic Chemistry, 2023, 26(4): e202200614.

4 She B X, Wan X J, Tang J N, et al. Sizeand morphologydependent antibacterial properties of cuprous oxide nanoparticle and their synergistic antibacterial effect J . Science of Advanced Materials, 2016, 8(5): 10741078.

5 Liang X D, Gao L, Yang S W, et al. Facile synthesis and shape evolution of singlecrystal cuprous oxide J . Advanced Materials, 2009, 21(20): 20682071.

6 Mukhtar M A, Syazana M S, Farhana A, et al. Review of various strategies to boost the photocatalytic activity of the cuprous oxidebased photocatalyst J . Journal of Environmental Chemical Engineering, 2021, 9(2): 105138.

7 ]万文亮 , 郎五可 , 郭晓伟 . 葡萄糖还原法制备不同形貌氧化亚铜的研究[ J . 化学研究与应用 , 2020, 32(7): 11411146.

8 ]张茂林 , 成蕊 . 纳米氧化亚铜的水热法制备及其可见光催化性能[ J . 淮北师范大学学报(自然科学版) , 2021, 42(4): 4246.

9 Zayed M F, Eisa W H, Anis B. Gallic acidassisted growth of cuprous oxide within polyvinyl alcohol; a separable catalyst for oxidative and reductive degradation of water pollutants J . Journal of Cleaner Production, 2021, 279: 123826.

10 ]莫若飞 . 多孔腔骰子形和六足形氧化亚铜的水热合成[ J . 材料导报 , 2020, 34(Z1): 148152.

相似文献/References:

[1]王元前,刘琳,姚菊明.溶剂热法制备碳纳米纤维负载Cu2O光催化材料[J].浙江理工大学学报,2013,30(02):7.
 WANG Yuan qian,LIU Lin,YAO Ju ming.Preparation of Carbon NanofiberLoaded Cu2O PhotocatalyticMaterials with Solvothermal Method[J].Journal of Zhejiang Sci-Tech University,2013,30(自科六):7.
[2]张明慧,杨伟柯,郑旭明.氧化亚铜的SiO 2复合改性及其抗菌性研究[J].浙江理工大学学报,2015,33-34(自科5):639.
 ZHANG Ming hui,YANG Wei ke,ZHENG Xu ming.Study on SiO 2 Compound Modification of Cuprous Oxideand Its Antibacterial Properties[J].Journal of Zhejiang Sci-Tech University,2015,33-34(自科六):639.

备注/Memo

备注/Memo:
收稿日期: 2023-02-08
基金项目: 浙江省基础公益研究计划项目(LGG21E030011);嘉兴市科技计划项目(2020AY10014)
作者简介: 张晓辉(1997-),男,浙江嘉兴人,硕士研究生,主要从事新纤维材料及功能性纤维材料方面的研究。
通信作者: 颜志勇,Email:yzyong77@zjxu.edu.cn
更新日期/Last Update: 2023-11-14