|本期目录/Table of Contents|

[1]许枭然,周璘,孙雪,等.银纳米粒子/聚多巴胺微球的制备及催化性能[J].浙江理工大学学报,2016,35-36(自科4):548-553.
 XU Xiaoran,ZHOU Lin,SUN Xue,et al.Preparation of Silver Nanoparticles /Polydopamine Nanosphere and Its Catalytic Property[J].Journal of Zhejiang Sci-Tech University,2016,35-36(自科4):548-553.
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银纳米粒子/聚多巴胺微球的制备及催化性能()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第35-36卷
期数:
2016年自科4期
页码:
548-553
栏目:
出版日期:
2016-07-10

文章信息/Info

Title:
Preparation of Silver Nanoparticles /Polydopamine Nanosphere and Its Catalytic Property
文章编号:
1673-3851 (2016) 04-0548-06
作者:
许枭然周璘孙雪刘吉洋奚凤娜
浙江理工大学理学院,杭州 310018
Author(s):
XU Xiaoran ZHOU Lin SUN Xue LIU Jiyang XI Fengna
School of Science, Zhejiang Sci-Tech University, Hangzhou 310018, China
关键词:
聚多巴胺银纳米粒子复合材料4 硝基苯酚催化还原
分类号:
O63.73
文献标志码:
A
摘要:
利用多巴胺在碱性醇/水体系中的氧化自聚反应制备得到粒径均一的聚多巴胺纳米微球(polydopamine spheres, PDS),并进一步利用PDS结构中儿茶酚胺的还原性,原位还原硝酸银负载银纳米粒子,建立了银纳米粒子/聚多巴胺微球(Ag nanoparticles loaded PDS, AgNPs/PDS)的简单制备方法。利用紫外可见光谱、傅里叶变换红外光谱、扫描电子显微镜、X射线光电子能谱和电化学溶出伏安法对PDS及AgNPs/PDS的形貌、结构及成分进行分析。在最优条件下,粒径约为40 nm的球形AgNPs均匀固载在平均粒径约为200 nm的PDS表面。通过紫外可见吸收光谱现场监测了AgNPs/PDS对硼氢化钠还原 4硝基苯酚(4nitrophenol,4NP)的催化作用,结果表明AgNPs/PDS极大地加速了4NP的还原反应。这种绿色、简单、快捷的复合材料制备方法有望为新型功能材料构建提供新途径。

参考文献/References:

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备注/Memo

备注/Memo:
收稿日期: 2015-09-21
基金项目: 国家自然科学基金项目(21305127);浙江省自然科学基金项目(Y15B050022)
作者简介: 许枭然(1990-),女,安徽蚌埠人,硕士研究生,主要从事功能材料制备及应用方面的研究
通信作者: 奚凤娜,E-mail:fengnaxi@zstu.edu.cn
更新日期/Last Update: 2016-09-13