[1]王盼,朱罕,包世勇,等.静电纺制备二氧化硅纳米管及其形貌调控的研究[J].浙江理工大学学报,2014,31-32(自科2):190-194.
WANG Pan,ZHU Han,BAO Shi yong,et al.Preparation of SiO 2 Nanotube by Electrospinning Method and Study of Its Morphology Control[J].Journal of Zhejiang Sci-Tech University,2014,31-32(自科2):190-194.
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静电纺制备二氧化硅纳米管及其形貌调控的研究(
)
WANG Pan,ZHU Han,BAO Shi yong,et al.Preparation of SiO 2 Nanotube by Electrospinning Method and Study of Its Morphology Control[J].Journal of Zhejiang Sci-Tech University,2014,31-32(自科2):190-194.
)浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]
- 卷:
- 第31-32卷
- 期数:
- 2014年自科2期
- 页码:
- 190-194
- 栏目:
- (自科)纺织与服装工程
- 出版日期:
- 2014-03-10
文章信息/Info
- Title:
- Preparation of SiO 2 Nanotube by Electrospinning Method and Study of Its Morphology Control
- 文章编号:
- 1673-3851 (2014) 02-0190-05
- 分类号:
- TB383
- 文献标志码:
- A
- 摘要:
- 以无水乙醇为溶剂,聚乙烯吡咯烷酮和正硅酸乙酯为原料,通过溶胶凝胶法制备纺丝前驱体,然后利用静电纺丝技术得到电纺纤维,再经煅烧处理后得到外径150 nm左右的二氧化硅纳米管。通过场发射扫描电子显微镜(FE SEM)和透射电子显微镜(TEM)研究电纺纤维和二氧化硅纳米管的形貌,利用傅里叶转换红外光谱(FT IR)和X 射线多晶粉末衍射仪(XRD)证明二氧化硅纳米管的形成。结果显示:当纺丝参数分别为电压10 kV、流速1.5 mL/h、接收距离14 cm,原料配方为:聚乙烯吡咯烷酮1.5 g、无水乙醇16 mL、正硅酸乙酯3.2 mL时,获得的电纺纤维和二氧化硅纳米管均具有良好的形貌。
参考文献/References:
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［2］ Wang W, Zhou J Y, Zhang S S, et al. A novel method to fabricate silica nanotubes based on phase separation effect［J］. J Mater Chem, 2010, 20: 9068-9072.
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［8］ 丁源维, 王騊, 姚菊明, 等. 静电纺制备TiO 2/PVA复合纳米纤维及其光催化性能研究［J］. 浙江理工大学学报, 2013, 30(1): 31-35.
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［11］ Zhang Z Y, Shao C L, Zou P, et al. In situ assembly of well dispersed gold nanoparticles on electrospun silica nanotubes for catalytic reduction of 4nitrophenol［J］. Chem Commun, 2011, 47: 3906-3908.
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备注/Memo
- 备注/Memo:
-
收稿日期： 2013-04-25
基金项目： 国家自然科学基金(51243001)
作者简介： 王盼(1989-),女,河南南阳人,硕士研究生,主要从事电纺纤维研究
通信作者： 杜明亮,电子邮箱:du@zstu.edu.cn
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