|本期目录/Table of Contents|

[1]Carrington M TAKAWIRA,虞雅伦,庄广清,等.二氧化硅气凝胶的常压低温快速制备和表征[J].浙江理工大学学报,2016,35-36(自科2):178-181.
 Carrington M TAKAWIRA,YU Yalun,ZHUANG Guangqing,et al.Fast Preparation of Inorganic Silica Aerogels Under Ambient  Pressure and Low Temperature and Its Representation[J].Journal of Zhejiang Sci-Tech University,2016,35-36(自科2):178-181.
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二氧化硅气凝胶的常压低温快速制备和表征()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第35-36卷
期数:
2016年自科2期
页码:
178-181
栏目:
出版日期:
2016-03-10

文章信息/Info

Title:
Fast Preparation of Inorganic Silica Aerogels Under Ambient  Pressure and Low Temperature and Its Representation
文章编号:
1673-3851 (2016) 02-0178-04
作者:
Carrington M TAKAWIRA虞雅伦庄广清 黄益邵建中
浙江理工大学,a.生态染整技术教育部工程研究中心;b.先进纺织材料与制备技术教育部重点实验室,杭州 310018
Author(s):
Carrington M TAKAWIRA YU Yalun ZHUANG Guangqing HUANG Yi SHAO Jianzhong
a.Engineering Research Center for Eco Dyeing and Finishing of Textiles, Ministry of Education; b. Key Laboratory of Advanced Textile and Manufactwring Technology, Ministry of Education, Zhejiang Sci-Tech University, Hangzhou 310018, China
关键词:
气凝胶溶胶凝胶溶剂置换表面改性
分类号:
TQ127.2
文献标志码:
A
摘要:
二氧化硅气凝胶凭借其极高的孔隙率和低导热性能已成为近年的热门研究材料之一。文章在常压低温条件下以正硅酸四乙酯为硅源,异丙醇和正己烷溶液为溶剂,通过低表面能溶剂置换以及粒子表面改性的方法快速制备无机气凝胶材料,并采用FESEM、HRTEM、FTIRATR光谱及X射线衍射分析等手段对所制备气凝胶材料的表观形貌、化学结构以及结晶性能进行表征。研究表明: 制得的二氧化硅气凝胶表面连有疏水的Si—CH 3基团、存在丰富的介孔结构,粒子和孔隙的尺寸较小,是一种孔隙率高、轻质、且热稳定性较高的微晶纳米材料,具有广泛的应用前景。

参考文献/References:

[1] PIERRE A C, PAJONK G M. Chemistry of aerogels and their applications[J]. Chemical Reviews, 2002, 102 (11): 4243-4266.
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[8] 胡银, 张和平, 黄冬梅, 等. 柔韧性块体疏水二氧化硅气凝胶的制备及表征[J]. 硅酸盐学报, 2013, (8): 1037-1041.
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[10] LI L, YALCIN B, NGUYEN B N, et al. Flexible nanofiber reinforced aerogel (xerogel) synthesis, manufacture, and characterization[J]. ACS Applied Materials & Interfaces, 2009, 1(11): 2491-2501.

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备注/Memo

备注/Memo:
收稿日期: 2015-06-06
作者简介: Carrington M. TAKAWIRA(1988-),男,津巴布韦人,硕士研究生,主要从事气凝胶制备方面的研究
通信作者: 邵建中,E-mail:jshao@zstu.edu.cn
更新日期/Last Update: 2016-06-01