|本期目录/Table of Contents|

[1]孟海丽,胡海华,沈洪磊,等. CdS空心球的制备及其光催化性能[J].浙江理工大学学报,2013,30(01):114-118.
 MENG Hai li,HU Hai hua,SHEN Hong lei,et al. Synthesis and Photocatalytic Activity of CdS Hollow Nanospheres[J].Journal of Zhejiang Sci-Tech University,2013,30(01):114-118.
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 CdS空心球的制备及其光催化性能()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第30卷
期数:
2013年01期
页码:
114-118
栏目:
生物与生命科学
出版日期:
2013-01-20

文章信息/Info

Title:
 Synthesis and Photocatalytic Activity of CdS Hollow Nanospheres
文章编号:
1673\|3851 (2013) 01\|0114\|05
作者:
 孟海丽1 胡海华2 沈洪磊1 唐为华3 崔灿1
 1. 浙江理工大学光电材料与器件中心, 杭州 310018;
2. 浙江大学城市学院, 杭州 310015; 
3. 北京邮电大学信息光子学与光通信国家重点实验室, 北京 100876
Author(s):
 MENG Haili1 HU Haihua2 SHEN Honglei1 TANG Weihua3 CUI Can1
 1. Center for Optoelectronics Materials and Devices, Department of Physics, Zhejiang SciTechUniversity, Hangzhou 310018, China;
2. City College, Zhejiang University, Hangzhou 310015, China;
3. State Key Laboratory of Information Photonics & Optical Communication, Beijing University Postsand Telecommunications, Beijing 100876, China
关键词:
 CdS 空心球 光催化
分类号:
O612
文献标志码:
A
摘要:
     以SiO2微球为模板,采用超声辅助法制备CdS空心球;探索了氨水用量对CdS壳层形成的影响,并从CdS壳层形成机制上解释了氨水的影响原因。利用电子能谱(EDX)、X射线衍射(XRD)、扫描电镜(SEM)、透射电镜(TEM)、荧光光谱(PL)、漫反射紫外可见光谱(DRUVS)测试手段研究了CdS空心球的成份、晶型、形貌及光学性能。结果表明:当氨水添加量为3.0 mL时,反应溶液中离子离子生长机制占主导地位,在该条件下制备了结晶良好的闪锌矿相CdS空心球,微球分散性良好,壳层致密稳定。光催化降解罗丹明B的结果表明,制备的CdS空心球具有优良的可见光催化性能。

参考文献/References:

[1] Esmaili M, HabibiYangjeh A. Microwaveassisted preparation of CdS nanoparticles in a halidefree ionic liquid and their photocatalytic activities[J]. Chinese Journal of Catalysis, 2011, 6(32): 933938.
[2] Lin G F, Zheng J W, Xu R. Templatefree synthesis of uniform CdS hollow nanospheres and their photocatalytic activities[J]. J Phys Chem C, 2008, 112(19): 73637370.
[3] Li X P, Gao Y N, Yu L, et al. Templatefree synthesis of CdS hollow nanospheres based on an ionic liquid assisted hydrothermal process and their application in photocatalysis[J]. Journal of Solid State Chemistry, 2010, 183: 14231432.
[4] Dai Z H, Zhang J, Bao J C, et al. Facile synthesis of highquality nanosized CdS hollow spheres and their application in electrogenerated chemiluminescence sensing[J]. J Mater Chem, 2007, 17: 10871093.
[5] Huang Y Y, Sun F Q, Wu T X, et al. Photochemical preparation of CdS hollow microspheres at room temperature and their use in visiblelight photocatalysis[J]. Journal of Solid State Chemistry, 2011, 184: 644648.
[6] Yu C L, Yu J C, Chan M. Sonochemical fabrication of fluorinated mesoporous titanium dioxide microspheres[J]. Journal of Solid State Chemistry, 2009, 182: 10611069.
[7] 谢荣国. 光子晶体用结构基元的制备、自组装与性能[D]. 杭州: 浙江大学, 2006.
[8] Song X F, Gao L. Fabrication of hollow hybrid microspheres coated with silica/titania via solgel process and enhanced photocatalytic activities[J]. J Phys Chem. C, 2007, 111(23): 81808187.
[9] Wu D Z, Ge X W, Zhang Z C, et al. Novel onestep route for synthesizing CdS/Polystyrene nanocomposite hollow spheres[J]. Langmuir, 2004, 20(13): 51925195.
[10] AlAni S K J, AlHassang I H O, AlDahan Z T. The opticalproperties and ac conductivity of magnesium phosphateglasses[J]. J Mater Sci, 1995, 30(14): 37203729.

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备注/Memo

备注/Memo:
收稿日期: 2011-12-06
基金项目: 浙江省教育厅科研项目(Y201223380),国家自然科学基金项目(60806045,11074220),浙江大学城市学院教师科研基金(J12009)
作者简介: 孟海丽(1985-),女,河南濮阳人,硕士研究生,主要从事功能纳米材料的制备与表征的研究。
通信作者: 崔灿,Email:cancui@zstu.edu.cn
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