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[1]侯锐刚a,b,易玲敏a,等. 含聚苯乙烯侧链的两亲性有机硅接枝共聚物的合成与表征[J].浙江理工大学学报,2011,28(06):831-835.
 HOU Rui ganga,b,YI Ling mina,et al. Synthesis and Characterization of Amphiphilic Silicone Graft Copolymers Containing Polystyrene SideChain[J].Journal of Zhejiang Sci-Tech University,2011,28(06):831-835.
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 含聚苯乙烯侧链的两亲性有机硅接枝共聚物的合成与表征()
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浙江理工大学学报[ISSN:1673-3851/CN:33-1338/TS]

卷:
第28卷
期数:
2011年06期
页码:
831-835
栏目:
纺织与材料
出版日期:
2011-12-30

文章信息/Info

Title:
 Synthesis and Characterization of Amphiphilic Silicone Graft Copolymers Containing Polystyrene SideChain
文章编号:
16733851 (2011) 06083105
作者:
侯锐刚ab 易玲敏ab 林鹤鸣ab 黄传霞ab
 浙江理工大学, a. 生态染整技术教育部工程研究中心; b. 先进纺织材料与制备技术教育部重点实验室, 杭州 310018
Author(s):
 HOU Ruigangab YI Lingminab LIN Hemingab HUANG Chuanxiaab
 Zhejiang SciTech University, a. Engineering Research Center for EcoDyeing & Finishing of Textiles, Ministry of Education; b. The Key Laboratory of Advanced Textile Materials and Manufacturing Technology, Ministry of Education, Hangzhou 310018, China
关键词:
 阴离子聚合 硅氢加成 聚苯乙烯 两亲性有机硅接枝共聚物
分类号:
O631
文献标志码:
A
摘要:
    在甲苯溶剂中,以正丁基锂(nBuLi)为引发剂,运用阴离子聚合制备端乙烯基聚苯乙烯大分子单体(VPS);在四氢呋喃(THF)溶剂中,通过含氢硅油与VPS、端烯丙基聚醚(APE)及烯丙基缩水甘油醚(AGE)的硅氢加成反应,合成了含聚苯乙烯(PS)侧链的两亲性有机硅接枝共聚物,并通过GPC、1HNMR、FTIR等测试手段对接枝共聚物结构进行了表征。所得聚合物可作为一种多功能型的有机颜料分散剂,用于颜料印花。

参考文献/References:

 [1] 周春隆, 穆振义. 有机颜料: 结构、特性及应用[M]. 北京: 化学工业出版社, 2002.
[2] Lelu S, Novat C, Graillat C, et al. Encapsulation of an organic phthalocyanine blue pigment into polystyrene latex particles using a miniemulsion polymerization process[J]. Polym Int, 2003, 52(4): 542547.
[3] Bulychev N A, Arutunov I A, Zubov V P, et al. Block copolymers of vinyl ethers as thermoresponsive colloidal stabilizers of organic pigments in aqueous media[J]. Macromol Chem Phys, 2004, 205(18): 24572463.
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[5] Auschra C, Eckstein E, Mühlebach A, et al. Design of new pigment dispersants by controlled radical polymerization[J]. Prog Org Coat, 2002, 45(23): 8393.
[6] Reuter E, Dr Silber S, Dr Psiorz C. The use of new blockcopolymeric dispersing agents for waterborne paints—theoretical and practical aspects[J]. Prog Org Coat, 1999, 37(3/4): 161167.
[7] Svitova T, Hoffmann H, Randal M. Hill. Trisiloxane surfactants: surface/interfacial tension dynamics and spreading on hydrophobic surfaces[J]. Langmuir, 1996, 12(7): 17121721.
[8] Riess G. Micellization of block copolymers[J]. Prog Polym Sci, 2003, 28(7): 11071170.
[9] Alexandridis P, Lindman B. Amphiphilic Block Copolymers: SelfAssembly and Applications[M]. Elsevier: Amsterdam, 2000.
[10] Masehke U, Wagner T, Coqueret X. Synthesis of highmolecularweight poly(dimethylsiloxnae) of uniform size by anionic polymerization, 1. initiation by a monofunctional lithium siloxanolate[J]. Macromol Chem Phys, 1992, 193(9): 24532466.

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备注/Memo

备注/Memo:
 收稿日期: 2010-11-30
基金项目: 国家自然科学基金(2060629);浙江省自然科学基金(Y4090579);浙江理工大学科研启动基金(0701652Y)
作者简介: 侯锐刚(1985-),男,陕西宝鸡人,硕士研究生,主要从事新型纺织化学品的合成研究。
通讯作者: 易玲敏,电子邮箱:lmyi@zstu.edu.cn
更新日期/Last Update: